Piperine – beilstein/crossfire reference list

Reference List

FAIDE(1); FLST(13); XREF(3); INP(6); CDER(2); MP(9); CRYPH(2); NMR(1); IR(1); UV(2); MS(1); POT(1); FINFO(2); RX(4); CNR(20)

Substance (1 of 1)

Beilstein Registry Number90739Beilstein Preferred RN94-62-2CAS Registry Number94-62-2; 495-91-0; 7780-20-3; 30511-76-3; 30511-77-4Chemical Name1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine; 1-Piperinoyl-piperidin; piperineAutoname5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-penta-2,4-dien-1-oneMolecular FormulaC17H19NO3Molecular Weight285.34Lawson Number24081; 22876Compound TypeheterocyclicConstitution ID38159Tautomer ID14686Beilstein Reference5-20-03-00469; 6-20Entry Date1988/06/27Update Date1994/01/18

Reference (1 of 20)

Citation Number119906Document TypeJournalAuthorsStoklosa,K.CODENBSCFASJournal TitleBull.Soc.Chim.Fr.Language CodeFRPublication Year1969Page3802-3806

Reference (2 of 20)

Citation Number2605306Document TypeJournalAuthorsLloyd et al.CODENJACSATJournal TitleJ.Amer.Chem.Soc.(Series) Volume82Publication Year1960Page3791

Reference (3 of 20)

Citation Number2835455Document TypeJournalAuthorsGupta et al.CODENPYTCASJournal TitlePhytochemistry(Series) Volume11Publication Year1972Page2646

Reference (4 of 20)

Citation Number3133321Document TypeJournalAuthorsDutta et al.CODENIJSBDBJournal TitleIndian J.Chem.Sect.B(Series) Volume15Publication Year1977Page583

Reference (5 of 20)

Citation Number3133481Document TypeJournalAuthorsLurik et al.CODENJGCHA4; ZOKHA4Journal TitleJ.Gen.Chem.USSR (Engl.Transl.); Zh.Obshch.Khim.(Series) Volume45; 45Publication Year1975; 1975Page2246; 2287

Reference (6 of 20)

Citation Number3141536Document TypeJournalAuthorsMazeau; ZarzyckiCODENCHDCAQJournal TitleC.R.Hebd.Seances Acad.Sci.Ser.C(Series) Volume281Publication Year1975Page583,584

Reference (7 of 20)

Citation Number3141959Document TypeJournalAuthorsLoder et al.CODENAJCHASJournal TitleAust.J.Chem.(Series) Volume22Publication Year1969Page1531,1538

Reference (8 of 20)

Citation Number3142215Document TypeJournalAuthorsBanerji; DharaCODENPYTCASJournal TitlePhytochemistry(Series) Volume13Publication Year1974Page2327

Reference (9 of 20)

Citation Number3142495Document TypeJournalAuthorsVashkov et al.CODENRZKHARJournal TitleRef.Zh.Khim.Journal/Review Without CODENChem.Abstr.(Series) Volume17; 81Number13234bPublication Year1973; 1974Page508

Reference (10 of 20)

Citation Number3214879Document TypeJournalAuthorsFeugeasCODENBSCFASJournal TitleBull.Soc.Chim.Fr.Publication Year1964Page1892

Reference (11 of 20)

Citation Number3220501Document TypeJournalAuthorsNormant; FeugeasCODENCOREAFJournal TitleC.R.Hebd.Seances Acad.Sci.(Series) Volume258Publication Year1964Page2846

Reference (12 of 20)

Citation Number3228104Document TypeJournalAuthorsGrahamCODENJPMSAEJournal TitleJ.Pharm.Sci.(Series) Volume54Publication Year1965Page319

Reference (13 of 20)

Citation Number3239881Document TypeJournalAuthorsMishra; TewariCODENJPMSAEJournal TitleJ.Pharm.Sci.(Series) Volume53Publication Year1964Page1423

Reference (14 of 20)

Citation Number3281384Document TypeJournalAuthorsTraxlerCODENJAFCAUJournal TitleJ.Agric.Food Chem.(Series) Volume19Publication Year1971Page1135,1137

Reference (15 of 20)

Citation Number3341233Document TypeJournalAuthorsSingh et al.CODENJICSAHJournal TitleJ.Indian Chem.Soc.(Series) Volume53Publication Year1976Page1162

Reference (16 of 20)

Citation Number3633748Document TypeJournalAuthorsBohnsackCODENRSARAQJournal TitleRiechst.Aromen(Series) Volume15Publication Year1965Page77

Reference (17 of 20)

Citation Number3678903Document TypeJournalAuthorsBordner; MullinsCODENCSCMCSJournal TitleCryst.Struct.Commun.(Series) Volume3Publication Year1974Page693

Reference (18 of 20)

Citation Number4815504Document TypeJournalAuthorsKulkaCODENJAFCAUJournal TitleJ.Agric.Food Chem.(Series) Volume15Publication Year1967Page48,51

Reference (19 of 20)

Citation Number5546680Document TypeJournalAuthorsMandai, Tadakatsu; Moriyama, Tadashi; Tsujimoto, Koichiro; Kawada, Mikio; Otera, JunzoCODENTELEAYJournal TitleTetrahedron Lett.Language CodeEN(Series) Volume27Number5Publication Year1986Page603-606

Reference (20 of 20)

Citation Number5686470Document TypeJournalAuthorsHoelzel, Claus; Spiteller, GerhardCODENLACHDLJournal TitleLiebigs Ann.Chem.Language CodeGENumber7Publication Year1984Page1319-1331

Reaction (1 of 4)

Reaction ID2627935Reactant BRN4613019Reactantacetic acid 1-(benzenesulfonyl-benzo[1,3]dioxol-5-yl-methyl)-4-oxo-4-piperidin-1-yl-butyl esterProduct BRN90739; 90741Product1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine; 1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationReagentt-BuOKSolvent2-methyl-propan-2-olTime12 hour(s)Other ConditionsAmbient temperatureCommentYield given. Yields of byproduct givenCitation Pointer5546680; Journal; Mandai, Tadakatsu; Moriyama, Tadashi; Tsujimoto, Koichiro; Kawada, Mikio; Otera, Junzo; TELEAY; Tetrahedron Lett.; EN; 27; 5; 1986; 603-606;

Reaction (2 of 4)

Reaction ID3863768Reactant BRN90739Reactant1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidineProduct BRN5564597Product5-(3,4-Dihydroxyphenyl)-2,4-pentadiensaeure-piperididNo. of Reaction Details1Reaction ClassificationPreparationYield86 percent (BRN=5564597)Reagent0.5 M BBr3, 0.5 M sodium acetate buffer (pH=5)SolventCH2Cl2Time72 hour(s)Other ConditionsAmbient temperatureCitation Pointer5686470; Journal; Hoelzel, Claus; Spiteller, Gerhard; LACHDL; Liebigs Ann.Chem.; GE; 7; 1984; 1319-1331;

Reaction (3 of 4)

Reaction ID5392514Reactant BRN90739Reactant1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidineNo. of Reaction Details2Reaction ClassificationChemical behaviour (half reaction)Subject StudiedKineticsCitation Pointer119906; Journal; Stoklosa,K.; BSCFAS; Bull.Soc.Chim.Fr.; FR; 1969; 3802-3806;

Reaction (4 of 4)

Reaction ID5714783Product BRN90739Product1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidineNo. of Reaction Details1Reaction ClassificationPreparation (half reaction)Citation Pointer3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;3214879; Journal; Feugeas; BSCFAS; Bull.Soc.Chim.Fr.; 1964; 1892;

Isolation from Natural Product (1 of 6)

Isolation from Natural Productaus Piper nigrum L.Citation Pointer3281384; Journal; Traxler; JAFCAU; J.Agric.Food Chem.; 19; 1971; 1135,1137;

Isolation from Natural Product (2 of 6)

Isolation from Natural Productaus PfefferCitation Pointer3633748; Journal; Bohnsack; RSARAQ; Riechst.Aromen; 15; 1965; 77;

Isolation from Natural Product (3 of 6)

Isolation from Natural Productaus Stengel von Piper nigrum Linn.Citation Pointer3341233; Journal; Singh et al.; JICSAH; J.Indian Chem.Soc.; 53; 1976; 1162;

Isolation from Natural Product (4 of 6)

Isolation from Natural Productaus Piper chabaCitation Pointer3239881; Journal; Mishra; Tewari; JPMSAE; J.Pharm.Sci.; 53; 1964; 1423;

Isolation from Natural Product (5 of 6)

Isolation from Natural Productaus Piper longum Linn.Citation Pointer3133321; Journal; Dutta et al.; IJSBDB; Indian J.Chem.Sect.B; 15; 1977; 583;

Isolation from Natural Product (6 of 6)

Isolation from Natural Productaus Piper nepalenseCitation Pointer2835455; Journal; Gupta et al.; PYTCAS; Phytochemistry; 11; 1972; 2646;

Derivative (1 of 2)

CommentHydrobromid: C17H19NO3*HBr: aus Piperin in Bzl., ges. benzol. HBr-Lsg.; F: 170gradCitation Pointer3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;

Derivative (2 of 2)

CommentHydrobromid: F: 170grad (aus Bzl.; Kofler-App:)Citation Pointer3214879; Journal; Feugeas; BSCFAS; Bull.Soc.Chim.Fr.; 1964; 1892;

Crossfile Reference (1 of 3)

NamePiperine; for synthesisCrossfile SourceE.Merck, DarmstadtExternal Access ID821036

Crossfile Reference (2 of 3)

NamePIPERINE, 97 PERCENTCrossfile SourceAldrichExternal Access IDP49007

Crossfile Reference (3 of 3)

NamepiperineCrossfile SourceEINECSExternal Access ID202-348-0

Melting Point (1 of 9)

Melting Point129.2 – 130.5Citation Pointer3281384; Journal; Traxler; JAFCAU; J.Agric.Food Chem.; 19; 1971; 1135,1137;

Melting Point (2 of 9)

Melting Point129Solventdiethyl etherCitation Pointer3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;3214879; Journal; Feugeas; BSCFAS; Bull.Soc.Chim.Fr.; 1964; 1892;

Melting Point (3 of 9)

Melting Point128Citation Pointer119906; Journal; Stoklosa,K.; BSCFAS; Bull.Soc.Chim.Fr.; FR; 1969; 3802-3806;

Melting Point (4 of 9)

Melting Point128 – 129.5Citation Pointer3142495; Journal; Vashkov et al.; RZKHAR; Ref.Zh.Khim.; 17; 1973; 508; Chem.Abstr.; 81; 13234b; 1974;3633748; Journal; Bohnsack; RSARAQ; Riechst.Aromen; 15; 1965; 77;

Melting Point (5 of 9)

Melting Point129 – 130Citation Pointer2835455; Journal; Gupta et al.; PYTCAS; Phytochemistry; 11; 1972; 2646;

Melting Point (6 of 9)

Melting Point128 – 129Citation Pointer4815504; Journal; Kulka; JAFCAU; J.Agric.Food Chem.; 15; 1967; 48,51;

Melting Point (7 of 9)

Melting Point127 – 129Citation Pointer3142215; Journal; Banerji; Dhara; PYTCAS; Phytochemistry; 13; 1974; 2327;

Melting Point (8 of 9)

Melting Point128 – 129Citation Pointer3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;

Melting Point (9 of 9)

Melting Point120 – 129Citation Pointer3341233; Journal; Singh et al.; JICSAH; J.Indian Chem.Soc.; 53; 1976; 1162;

Crystal Phase (1 of 2)

DescriptionCrystal habitCitation Pointer3678903; Journal; Bordner; Mullins; CSCMCS; Cryst.Struct.Commun.; 3; 1974; 693;

Crystal Phase (2 of 2)

DescriptionCrystal growthCitation Pointer3141536; Journal; Mazeau; Zarzycki; CHDCAQ; C.R.Hebd.Seances Acad.Sci.Ser.C; 281; 1975; 583,584;

Nuclear Magnetic Resonance (1 of 1)

DescriptionNMRCitation Pointer3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;

Infrared Spectra (1 of 1)

DescriptionIRCitation Pointer3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;3142215; Journal; Banerji; Dhara; PYTCAS; Phytochemistry; 13; 1974; 2327;3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;

Ultraviolet Spectra (1 of 2)

DescriptionAbsorption maximaCitation Pointer3220501; Journal; Normant; Feugeas; COREAF; C.R.Hebd.Seances Acad.Sci.; 258; 1964; 2846;

Ultraviolet Spectra (2 of 2)

DescriptionUV/VISCitation Pointer3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;3281384; Journal; Traxler; JAFCAU; J.Agric.Food Chem.; 19; 1971; 1135,1137;

Mass Spectrum (1 of 1)

Citation Pointer3142215; Journal; Banerji; Dhara; PYTCAS; Phytochemistry; 13; 1974; 2327;

Electrochemical Characteristics (1 of 1)

Descriptionpolarographic half-wave potentialCitation Pointer3133481; Journal; Lurik et al.; JGCHA4; J.Gen.Chem.USSR (Engl.Transl.); 45; 1975; 2246; ZOKHA4; Zh.Obshch.Khim.; 45; 1975; 2287;

Further Information (1 of 2)

Citation Pointer3141959; Journal; Loder et al.; AJCHAS; Aust.J.Chem.; 22; 1969; 1531,1538;3228104; Journal; Graham; JPMSAE; J.Pharm.Sci.; 54; 1965; 319;

Further Information (2 of 2)

Citation Pointer2605306; Journal; Lloyd et al.; JACSAT; J.Amer.Chem.Soc.; 82; 1960; 3791;

FAIDE(1); FLST(23); XREF(4); RSTR(1); INP(30); CDER(1); CPD(2); MP(19); CRYPH(8); SP(1); DEN(4); DV(1); RI(1); NMR(15); IR(12); UV(10); MS(5); ELE(1); DE(3); POT(1); SLB(8); BSPM(1); PHARM(60); RX(31); CNR(126)

Substance (1 of 1)

Beilstein Registry Number90741Beilstein Preferred RN94-62-2CAS Registry Number94-62-2; 495-91-0; 7780-20-3; 30511-76-3; 30511-77-4Chemical Name1-trans,trans-piperinoyl-piperidine; piperine; (E,E)-1-[5-(1,3-benzodioxol-5-yl)-1-oxo-2,4-pentadienyl]-piperidineAutoname5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-penta-2,4-dien-1-oneMolecular FormulaC17H19NO3Molecular Weight285.34Lawson Number24081; 22876Structure KeywordStereo compoundCompound TypeheterocyclicConstitution ID38159Tautomer ID18563Beilstein Reference0-20-00-00079; 1-20-00-00023; 2-20-00-00053; 4-20-00-01341; 5-20-03-00469; 6-20Entry Date1988/06/27Update Date2002/04/29

Reference (1 of 126)

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Reaction (1 of 31)

Reaction ID1746488Reactant BRN4327482; 1310620Reactant2-(3,6-diisopropyl-pyrazine-2-sulfinyl)-1-piperidin-1-yl-ethanone; 5-(3-bromo-1-propenyl)-1,3-dioxaindanProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationReagent1.) potassium diisopropylamide (KDA)Other Conditions1.) THF, hexane, RT, 1 h, 2.) THF, hexane, refluxCommentYield given. Multistep reactionCitation Pointer5535863; Journal; Ohta, Akihiro; Tonomura, Yoshiko; Sawaki, Junko; Naohito, Sato; Akiike, Hitomi; et al.; HTCYAM; Heterocycles; EN; 32; 5; 1991; 965-973;

Reaction (2 of 31)

Reaction ID1748676Reactant BRN1365055; 131691ReactantN-2-butenoylpiperidine; benzo[1,3]dioxole-5-carbaldehydeProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details3Reaction ClassificationChemical behaviourReagenttriethylbenzylammoniumchloride, 50percent KOHSolventdimethylsulfoxideTime2 hour(s)Temperature60 – 65Other Conditionsvarious solventsSubject StudiedProduct distributionCitation Pointer5623047; Journal; Schulze, Andreas; Oediger, Hermann; LACHDL; Liebigs Ann.Chem.; GE; 9; 1981; 1725-1727;

Reaction (3 of 31)

Reaction ID1839034Reactant BRN167676; 4416084Reactant1-benzo[1,3]dioxol-5-yl-allyl alcohol; 1-p-tolylsulfanylethynyl-piperidineProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationOther Conditions1.) BF3OEt2 in refluxing toluene; 2.) oxidation (m-chloroperbenzoic acid, CH2Cl2,-78 grad C); 3.) reflux in tolueneCommentYield given. Multistep reactionCitation Pointer5542826; Journal; Nakai, Takeshi; Setoi, Hiroyuki; Kageyama, Yasuhide; TELEAY; Tetrahedron Lett.; EN; 22; 41; 1981; 4097-4100;

Reaction (4 of 31)

Reaction ID2627935Reactant BRN4613019Reactantacetic acid 1-(benzenesulfonyl-benzo[1,3]dioxol-5-yl-methyl)-4-oxo-4-piperidin-1-yl-butyl esterProduct BRN90739; 90741Product1-(5-benzo[1,3]dioxol-5-yl-penta-2,4-dienoyl)-piperidine; 1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationReagentt-BuOKSolvent2-methyl-propan-2-olTime12 hour(s)Other ConditionsAmbient temperatureCommentYield given. Yields of byproduct givenCitation Pointer5546680; Journal; Mandai, Tadakatsu; Moriyama, Tadashi; Tsujimoto, Koichiro; Kawada, Mikio; Otera, Junzo; TELEAY; Tetrahedron Lett.; EN; 27; 5; 1986; 603-606;

Reaction (5 of 31)

Reaction ID3829573Reactant BRN85624; 102438Reactanttrans,trans-piperinic acid; piperidineProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details2Reaction ClassificationPreparationYield90 percent (BRN=90741)ReagentN,N-bis(2-oxo-3-oxazolidinyl)phosphorodiamidic chloride, triethylamineSolventCH2Cl2Time60 minTemperature20 – 25Citation Pointer5571390; Journal; Cabre, Juan; Palomo, Antonio Luis; SYNTBF; Synthesis; EN; 5; 1984; 413-417;

Reaction (6 of 31)

Reaction ID3829578Reactant BRN85625; 102438Reactant5t-benzo[1,3]dioxol-5-yl-penta-2t,4-dienoyl chloride; piperidineProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details2Reaction ClassificationPreparationSolventdiethyl etherCitation Pointer5576619; Journal; Banerji, Avijit; Ghosal, Tapasree; Acharyya, Aditi K.; IJSBDB; Indian J.Chem.Sect.B; EN; 23; 6; 1984; 546-549;

Reaction (7 of 31)

Reaction ID3863772Reactant BRN1101343; 90741Reactantchloromalonic acid diethyl ester; 1-trans,trans-piperinoyl-piperidineProduct BRN1805352; 4894122Productethenetetracarboxylic acid tetraethyl ester; 3-benzo[1,3]dioxol-5-yl-6-(piperidine-1-carbonyl)-3,6-dihydro-selenopyran-2,2-dicarboxylic acid diethyl esterNo. of Reaction Details1Reaction ClassificationPreparationYield24 percent (BRN=4894122); 70 percent (BRN=1805352)Reagentselenium, Cs2CO3SolventacetonitrileOther ConditionsHeatingCitation Pointer5597332; Journal; Abelman, Matthew M.; TELEAY; Tetrahedron Lett.; EN; 32; 50; 1991; 7389-7392;

Reaction (8 of 31)

Reaction ID3863773Reactant BRN1101343; 90741Reactantchloromalonic acid diethyl ester; 1-trans,trans-piperinoyl-piperidineProduct BRN4894108Product3-benzo[1,3]dioxol-5-yl-6-(piperidine-1-carbonyl)-3,6-dihydro-thiopyran-2,2-dicarboxylic acid diethyl esterNo. of Reaction Details1Reaction ClassificationPreparationYield80 percent (BRN=4894108)Reagentsulfur, Cs2CO3SolventacetonitrileOther ConditionsHeatingCitation Pointer5597332; Journal; Abelman, Matthew M.; TELEAY; Tetrahedron Lett.; EN; 32; 50; 1991; 7389-7392;

Reaction (9 of 31)

Reaction ID3863774Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN110253Product1-nitroso-piperidineNo. of Reaction Details2Reaction ClassificationPreparationYield2.36 percent (BRN=110253)ReagentHClO4 (pH 3.0), NaNO2SolventH2OTime2 hour(s)Temperature100Citation Pointer5874363; Journal; Nakamura, Masamichi; Katoh, Kuni; Kawabata, Toshiharu; ABCHA6; Agric.Biol.Chem.; EN; 45; 5; 1981; 1257-1260;

Reaction (10 of 31)

Reaction ID3863775Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN288703Product1-(5-benzo[1,3]dioxol-5-yl-pentanoyl)-piperidineNo. of Reaction Details4Reaction ClassificationPreparationReagentH2Catalyst10 percent Pd/CSolventmethanolTime2 hour(s)Pressure2585.74Reaction TypeCatalytic hydrogenationCitation Pointer6262921; Journal; Ablordeppey, Seth Y.; Fischer, James B.; Glennon, Richard A.; BMECEP; Bioorg.Med.Chem.; EN; 8; 8; 2000; 2105 – 2112;

Reaction (11 of 31)

Reaction ID3863776Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN6144494; 6168367ProductZ-5-benzylidene-(3,4-methylenedioxy)-2(5H)-furanone; E,E-piperylpiperidine dimerNo. of Reaction Details3Reaction ClassificationChemical behaviourYield26 percent (BRN=6144494); 30 percent (BRN=6168367)Reagentrose bengalSolventmethanolTime18 hour(s)Other ConditionsIrradiationSubject StudiedMechanismCitation Pointer5753488; Journal; Kumar, Anil; Krupadanam, G L David; Srimannarayana, G; IJSBDB; Indian J.Chem.Sect.B; EN; 31; 11; 1992; 784-785;

Reaction (12 of 31)

Reaction ID3863777Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN6662570Product4,5-(trans)-2,3-epoxy piperylpiperidineNo. of Reaction Details1Reaction ClassificationPreparationYield75 percent (BRN=6662570)Reagent1percent H2O2Time18 hour(s)Temperature37Other ConditionsHorseradish peroxidase, 0,1M sodium phosphate buffer, pH 6,5Citation Pointer5851492; Journal; Rao, A. Bhaskar; Rao, M. Venkateswara; Kumar, Anil; Krupadanam, G. L. David; Srimannarayana, G.; TELEAY; Tetrahedron Lett.; EN; 35; 2; 1994; 279-280;

Reaction (13 of 31)

Reaction ID3863778Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN85624Producttrans,trans-piperinic acidNo. of Reaction Details3Reaction ClassificationPreparationReagent10percent ethanolic NaOHSolventethanolCitation Pointer5725528; Journal; Nakamura, Norio; Kiuchi, Fumiyuki; Tsuda, Yoshisuke; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2647-2651;

Reaction (14 of 31)

Reaction ID4925582Reactant BRN7989620; 114442Reactant5-(2-iodo-vinyl)-benzo[1,3]dioxole; 1-acryloyl-piperidineProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationYield38 percent (BRN=90741)Reagentpalladium acetate, triphenylphosphine, lithium chloride, triethylamineSolventacetonitrileTime18 hour(s)Temperature70 – 80Citation Pointer6096589; Journal; Naskar, Dinabandhu; Chowdhury, Shantanu; Roy, Sujit; TELEAY; Tetrahedron Lett.; EN; 39; 7; 1998; 699-702;

Reaction (15 of 31)

Reaction ID4975527Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN8003486; 288703Product5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-pent-4-en-1-one; 1-(5-benzo[1,3]dioxol-5-yl-pentanoyl)-piperidineNo. of Reaction Details1Reaction ClassificationPreparationYield58 percent (BRN=288703); 14 percent (BRN=8003486)ReagentNaBH4 (0.008 mole), I2 (0.003 mole)SolventtetrahydrofuranTime20 minTemperature0Citation Pointer6096582; Journal; Das, Biswanath; Kashinatham, A.; Madhusudhan, P.; TELEAY; Tetrahedron Lett.; EN; 39; 7; 1998; 677-678;

Reaction (16 of 31)

Reaction ID4975528Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN8003486Product5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-pent-4-en-1-oneNo. of Reaction Details1Reaction ClassificationPreparationYield74 percent (BRN=8003486)ReagentNaBH4 (0.0025 mole), I2 (0.001 mole)SolventtetrahydrofuranTime20 minTemperature0Citation Pointer6096582; Journal; Das, Biswanath; Kashinatham, A.; Madhusudhan, P.; TELEAY; Tetrahedron Lett.; EN; 39; 7; 1998; 677-678;

Reaction (17 of 31)

Reaction ID5043968Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN8117956; 1261487Product5-benzo[1,3]dioxol-5-yl-1-piperidin-1-yl-pent-3-en-1-one; trans-Db,g-Dihydro-piperidinNo. of Reaction Details1Reaction ClassificationPreparationYield95 percent (BRN=1261487)ReagentZn, HOAcTime2 hour(s)Other ConditionsAmbient temperatureCitation Pointer6117787; Journal; Das, Biswanath; Madhusudhan, P.; TELEAY; Tetrahedron Lett.; EN; 39; 49; 1998; 9099-9100;

Reaction (18 of 31)

Reaction ID5311563Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN1261487Producttrans-Db,g-Dihydro-piperidinNo. of Reaction Details1Reaction ClassificationPreparationYield96 percent (BRN=1261487)ReagentMg; MeOHTime2 hour(s)Temperature20Reaction TypeReductionCitation Pointer6209404; Journal; Das, Biswanth; Kashinatham, A.; Venkataiah, B.; SYNCAV; Synth.Commun.; EN; 29; 21; 1999; 3799 – 3804;

Reaction (19 of 31)

Reaction ID5392515Reactant BRN1238185; 90741Reactantbenzophenone; 1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationChemical behaviour (half reaction)Other Conditionsim LichtCommentHandbookCitation Pointer745868; Journal; Paterno; GCITA9; Gazz.Chim.Ital.; 44 II; 1914; 104, 106;

Reaction (20 of 31)

Reaction ID5680972Reactant BRN90741; 1718733Reactant1-trans,trans-piperinoyl-piperidine; ethanol; phenylmercury-acetateProduct BRN53813Product1-[5t-(6-phenylmercurio-benzo[1,3]dioxol-5-yl)-penta-2t,4-dienoyl]-piperidineNo. of Reaction Details2Reaction ClassificationPreparationCommentHandbookCitation Pointer784769; Patent; Lever Brothers Co.; US 2085064; 1935;

Reaction (21 of 31)

Reaction ID5709607Reactant BRN90741Reactantalcoholic KOH-solution; 1-trans,trans-piperinoyl-piperidineProduct BRN102438; 85624Productpiperidine; trans,trans-piperinic acidNo. of Reaction Details1Reaction ClassificationChemical behaviourCommentHandbookCitation Pointer960841; Journal; v. Babo; Keller; JPCEAO; J.Prakt.Chem.; <1> 72; 1857; 55; JCVWAE; Jahresber.Fortschr.Chem.Verw.Theile Anderer Wiss.; 1857; 413;503101; Journal; Fittig; Mielck; JLACBF; Justus Liebigs Ann. Chem.; 152; 1869; 52, 54; JLACBF; Justus Liebigs Ann. Chem.; 172; 1874; 140, 152;

Reaction (22 of 31)

Reaction ID5714786Product BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparation (half reaction)Citation Pointer3132215; Journal; Tsuboi; Takeda; TELEAY; Tetrahedron Lett.; 1979; 1043;3140982; Journal; Grewe et al.; CHBEAM; Chem.Ber.; 103; 1970; 3752,3766;3141492; Journal; Lurik et al.; PCJOAU; Pharm.Chem.J.(Engl.Transl.); 5; 8; 1971; 462; KHFZAN; Khim.Farm.Zh.; 5; 8; 1971; 15;2995721; Patent; Haarmann and Reimer; DE 2757506; 1977;

Reaction (23 of 31)

Reaction ID5714787Reactant BRN102438Reactantchavicinoyl chloride; piperidineProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationCommentHandbookCitation Pointer520054; Journal; Lohaus; Gall; JLACBF; Justus Liebigs Ann. Chem.; 517; 1935; 278, 284;507531; Journal; Lohaus; JPCEAO; J.Prakt.Chem.; <2> 119; 1928; 258;

Reaction (24 of 31)

Reaction ID5714788Reactant BRN102438Reactantpiperidine; piperinic acid chlorideProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationReagentbenzeneCommentHandbookCitation Pointer960844; Journal; Ruegheimer; CHBEAM; Chem.Ber.; 15; 1882; 1391;

Reaction (25 of 31)

Reaction ID5746581Reactant BRN1718733; 90741Reactantethanol; hydrogen; colloidal palladium; 1-trans,trans-piperinoyl-piperidineProducttetrahydropiperineNo. of Reaction Details1Reaction ClassificationChemical behaviour (half reaction)CommentHandbookCitation Pointer505033; Journal; Borsche; CHBEAM; Chem.Ber.; 44; 1911; 2945;967599; Journal; Skita; Meyer; CHBEAM; Chem.Ber.; 45; 1912; 3586;1310037; Journal; Paal; CHBEAM; Chem.Ber.; 45; 1912; 2226;

Reaction (26 of 31)

Reaction ID5746582Reactant BRN1098214; 90741Reactanthydrogen; hydrochloric acid; palladium chloride; 1-trans,trans-piperinoyl-piperidineProducttetrahydropiperineNo. of Reaction Details1Reaction ClassificationChemical behaviour (half reaction)CommentHandbookCitation Pointer621663; Journal; Skita; Franck; CHBEAM; Chem.Ber.; 44; 1911; 2866;

Reaction (27 of 31)

Reaction ID5746583Reactant BRN1098214; 90741Reactanthydrogen; hydrochloric acid; platinum chlorides; 1-trans,trans-piperinoyl-piperidineProducttetrahydropiperineNo. of Reaction Details1Reaction ClassificationChemical behaviour (half reaction)CommentHandbookCitation Pointer621663; Journal; Skita; Franck; CHBEAM; Chem.Ber.; 44; 1911; 2866;

Reaction (28 of 31)

Reaction ID8539764Reactant BRN84600; 114442Reactant3-benzo[1,3]dioxol-5-yl-acrylic acid; 1-acryloyl-piperidineProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationMultistageYield51 percent (BRN=90741)No. of Stages2Stage 1 Stage 2 Stage Reactant BRN114442Stage Reactant1-acryloyl-piperidineReagentN-bromosuccinimide; tetrabutylammonium trifluoroacetate; Pd(OAc)2; Ph3Sb; Et3NSolvent1,2-dichloro-ethane; 1,2-dichloro-ethaneTime4 hour(s); 20 hour(s)Temperature20Reaction TypeDecarboxylation; bromination; Hunsdiecker reaction; Heck reactionCitation Pointer6225104; Journal; Naskar, Dinabandhu; Roy, Sujit; TETRAB; Tetrahedron; EN; 56; 10; 2000; 1369 – 1378;

Reaction (29 of 31)

Reaction ID8735157Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN8705257Product1-[1-(3,4-methylenedioxyphenyl)-2,4-pentadienyl]piperidineNo. of Reaction Details1Reaction ClassificationPreparationReagentLiAlH4Solventdiethyl etherTime24 hour(s)Other ConditionsHeatingReaction TypeReductionCitation Pointer6262921; Journal; Ablordeppey, Seth Y.; Fischer, James B.; Glennon, Richard A.; BMECEP; Bioorg.Med.Chem.; EN; 8; 8; 2000; 2105 – 2112;

Reaction (30 of 31)

Reaction ID8900343Reactant BRN7622; 2811397; 102438Reactant3,4-methylenedioxy-trans-cinnamaldehyde; (triphenylphosphoranylidene)ethenone; piperidineProduct BRN90741Product1-trans,trans-piperinoyl-piperidineNo. of Reaction Details1Reaction ClassificationPreparationYield90 percent (BRN=90741)SolventtetrahydrofuranTime24 hour(s)Other ConditionsHeatingCitation Pointer6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 – 2397;

Reaction (31 of 31)

Reaction ID8986873Reactant BRN90741Reactant1-trans,trans-piperinoyl-piperidineProduct BRN8998762Product(5-benzo[1,3]dioxol-5-yl-thiophen-2-yl)-piperidin-1-yl-methanoneNo. of Reaction Details1Reaction ClassificationPreparationYield23 percent (BRN=8998762)Reagentnaphthalene-1,8-trisulfide-2-oxideSolventchlorobenzeneTime16 hour(s)Other ConditionsHeatingCitation Pointer6320341; Journal; Grainger, Richard S.; Procopio, Alberto; Steed, Jonathan W.; ORLEF7; Org.Lett.; EN; 3; 22; 2001; 3565 – 3568;

Isolation from Natural Product (1 of 30)

Isolation from Natural Productoleoresin, extract from fruits of Piper nigrum L. (Piperaceae)Citation Pointer6303567; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 2; 2001; 176 – 179;

Isolation from Natural Product (2 of 30)

Isolation from Natural Productstems of Piper tuberculatumCitation Pointer6264052; Journal; Navickiene, Hosana Maria D.; Alecio, Alberto Camilo; Kato, Massuo Jorge; Bolzani, Vanderlan da S.; Young, Maria Claudia M.; Cavalheiro, Alberto Jose; Furlan, Maysa; PYTCAS; Phytochemistry; EN; 55; 2410; 2000; 621 – 626;

Isolation from Natural Product (3 of 30)

Isolation from Natural Productdry fruits of black pepperCitation Pointer6225880; Journal; Paula, Vanderlucia F. de; A Barbosa, Luiz C. de; Demuner, Antonio J.; Pilo-Veloso, Dorila; Picanco, Marcelo C.; PMSCFC; Post Manage.Sci.; EN; 56; 2; 2000; 168 – 174;

Isolation from Natural Product (4 of 30)

Isolation from Natural Productfruits of Piper retrofractum Vahl.Citation Pointer6205590; Journal; Pande, Archana; Shukla, Y. N.; Srivastava, Ritu; Verma, Monika; IJSBDB; Indian J.Chem.Sect.B; EN; 36; 4; 1997; 377 – 379;

Isolation from Natural Product (5 of 30)

Isolation from Natural Productthe fruits of Piper Longum Linn (Piperaceae)Citation Pointer6161595; Journal; Das, B.; Kashinatham, A.; Madhusudhan, P.; BCFAAI; Boll.Chim.Farm.; EN; 137; 8; 1998; 319 – 320;

Isolation from Natural Product (6 of 30)

Isolation from Natural Productleaves of Piper betleCitation Pointer6124808; Journal; Parmar, Virinder S.; Jain, Subhash C.; Gupta, Sangita; Talwar, Sangeeta; Rajwanshi, Vivek K.; et al.; PYTCAS; Phytochemistry; EN; 49; 4; 1998; 1069-1078;

Isolation from Natural Product (7 of 30)

Isolation from Natural Productstems and leaves of Piper khasiana, Piper thomsoni, Piper acutislegnumCitation Pointer6124808; Journal; Parmar, Virinder S.; Jain, Subhash C.; Gupta, Sangita; Talwar, Sangeeta; Rajwanshi, Vivek K.; et al.; PYTCAS; Phytochemistry; EN; 49; 4; 1998; 1069-1078;

Isolation from Natural Product (8 of 30)

Isolation from Natural ProductPiper acutisleginum, Piperle, Piper khasianaCitation Pointer6080863; Journal; Parmar, Virinder S.; Jain, Subhash C.; Bisht, Kirpal S.; Jain, Pajni; Taneja, Poonam; et al.; PYTCAS; Phytochemistry; EN; 46; 4; 1997; 597-674;

Isolation from Natural Product (9 of 30)

Isolation from Natural Productfruits of Piper nigrumCitation Pointer6070238; Journal; Siddiqui, Bina S.; Begum, Sabira; Gulzar, Tahsin; Noor, Farhat and Fatima; PYTCAS; Phytochemistry; EN; 45; 8; 1997; 1617-1620;

Isolation from Natural Product (10 of 30)

Isolation from Natural Productfruits of Piper longum L. (Piperaceae), climber from IndiaCitation Pointer6049858; Journal; Das, Biswanath; Kashinatham, A.; Srinivas, K. V. N. S.; PLMEAA; Planta Med.; EN; 62; 6; 1996; 582;

Isolation from Natural Product (11 of 30)

Isolation from Natural Productblack pepper at 294 bar and 42 deg C, extracted with CO2Citation Pointer5945187; Journal; Braumann, Urich; Haendel, heidrun; Albert, Klaus; Ecker, Rainer; Spraul, Manfred; ANCHAM; Anal.Chem.; EN; 67; 5; 1995; 930-935;

Isolation from Natural Product (12 of 30)

Isolation from Natural Productfruits of white pepper (Piper nigrum L.)Citation Pointer5874394; Journal; Nakatani, Nobuji; Inatani, Reiko; ABCHA6; Agric.Biol.Chem.; EN; 45; 6; 1981; 1473-1476;

Isolation from Natural Product (13 of 30)

Isolation from Natural ProductPiper nigrum L.Citation Pointer5874363; Journal; Nakamura, Masamichi; Katoh, Kuni; Kawabata, Toshiharu; ABCHA6; Agric.Biol.Chem.; EN; 45; 5; 1981; 1257-1260;

Isolation from Natural Product (14 of 30)

Isolation from Natural ProductUlocladium sp.Citation Pointer5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;

Isolation from Natural Product (15 of 30)

Isolation from Natural Productfruits of Javanese long pepper, Piper retrofractum Vahl.Citation Pointer5846053; Journal; Kikuzaki, Hiroe; Kawabata, Marona; Ishida, Etsuko; Akazawa, Yoko; Takei, Yoko; et al.; BBBIEJ; Biosci.Biotechnol.Biochem.; EN; 57; 8; 1993; 1329-1333;

Isolation from Natural Product (16 of 30)

Isolation from Natural ProductAnethum sowa (seeds)Citation Pointer5749938; Journal; Jain, A. K.; Sharma, N. D.; Gupta, S. R.; IJSBDB; Indian J.Chem.Sect.B; EN; 25; 1986; 979;

Isolation from Natural Product (17 of 30)

Isolation from Natural Productpepper, fruits of Piper nigrum L.Citation Pointer5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Isolation from Natural Product (18 of 30)

Isolation from Natural ProductPiper retrofractum (Piperaceae)Citation Pointer5710925; Journal; Ahn, Jong-Woong; Ahn, Mi-Ja; Zee, Ok-Pyo; Kim, Eun-Joo; Lee, Sueg-Geun; et al.; PYTCAS; Phytochemistry; EN; 31; 10; 1992; 3609-3612;

Isolation from Natural Product (19 of 30)

Isolation from Natural Productfruits of Piper longum L.Citation Pointer5673694; Journal; Tabuneng, Wnanbyr; Bando, Hideo; Amiya, Takashi; CPBTAL; Chem.Pharm.Bull.; EN; 31; 10; 1983; 3562-3565;

Isolation from Natural Product (20 of 30)

Isolation from Natural ProductPiper argyrophyllum Miq.Citation Pointer5575872; Journal; Banerji, Avijit; Nandi, Gopa; IJSBDB; Indian J.Chem.Sect.B; EN; 27; 1-12; 1988; 163-165;

Isolation from Natural Product (21 of 30)

Isolation from Natural ProductPiper nigrum L.Citation Pointer5510783; Journal; Das, B. P.; Jamal, Molla Yousuf; Choudhury, B.; JICSAH; J.Indian Chem.Soc.; EN; 67; 1; 1990; 72-73;

Isolation from Natural Product (22 of 30)

Isolation from Natural ProductVork. u. Isol. aus Piper peepuloidesCitation Pointer3143698; Journal; Dhar; Raina; PLMEAA; Planta Med.; 23; 1973; 295,296;

Isolation from Natural Product (23 of 30)

Isolation from Natural Productaus schwarzem PfefferCitation Pointer3141492; Journal; Lurik et al.; PCJOAU; Pharm.Chem.J.(Engl.Transl.); 5; 8; 1971; 462; KHFZAN; Khim.Farm.Zh.; 5; 8; 1971; 15;

Isolation from Natural Product (24 of 30)

Isolation from Natural Productaus Papaver aurantiacumCitation Pointer3132150; Journal; Madhusudhana et al.; CUSCAM; Curr.Sci.; 43; 1974; 76;

Isolation from Natural Product (25 of 30)

Isolation from Natural Productaus Fruechten von Piper guineenseCitation Pointer156361; Journal; Okogun,J.I.; Ekong,D.E.U.; JCPRB4; J.Chem.Soc.Perkin Trans.1; EN; 1974; 2195-2198;

Isolation from Natural Product (26 of 30)

Isolation from Natural ProductFindet sich in den unreifen Fruechten (‘schwarzer Pfeffer’) und in den Kernen der reifen Fruechte (‘weisser Pfeffer’) von Piper nigrumCommentHandbookCitation Pointer960850; Journal; Varrentrapp; Will; JLACBF; Justus Liebigs Ann. Chem.; 39; 1841; 283;960851; Journal; Regnault; ANCPAC; Ann.Chim.(Paris); <2> 68; 1838; 158;960852; Journal; Liebig; JLACBF; Justus Liebigs Ann. Chem.; 6; 1833; 36;960853; Journal; Pelletier; ANCPAC; Ann.Chim.(Paris); <2> 51; 1832; 199; JLACBF; Justus Liebigs Ann. Chem.; 6; 1833; 33;960854; Journal; Pelletier; ANCPAC; Ann.Chim.(Paris); <2> 16; 1821; 344; Schw.; 32; 436;960855; Journal; Oerstedt; Schweiggers Journ. f. Chemie u. Physik; 29; 80;

Isolation from Natural Product (27 of 30)

Isolation from Natural ProductFindet sich ferner im langen Pfeffer (reife Fruechte von P. longum und P. officinarum)CommentHandbookCitation Pointer960848; Journal; Wangerin; Pharm. Ztg.; 48; 454;960849; Journal; Bauer; Hilger; CHZEA6; Chem.Zentralbl.; GE; 67; I; 1896; 1214;

Isolation from Natural Product (28 of 30)

Isolation from Natural Productin den Fruechten von P. Clusii (Aschantipfeffer)CommentHandbookCitation Pointer960846; Journal; Herlant; PHJOAV; Pharm.J.; <3> 25; 643;960847; Journal; Stenhouse; PHJOAV; Pharm.J.; <1> 14; 363; JLACBF; Justus Liebigs Ann. Chem.; 95; 1855; 106;

Isolation from Natural Product (29 of 30)

Isolation from Natural Productin der Wurzelrinde von Artanthe geniculata (unechte Jaborandi)CommentHandbookCitation Pointer960845; Journal; Peckolt; Apoth. Ztg.; 10; 471;

Isolation from Natural Product (30 of 30)

Isolation from Natural Productin den Fruechten von P. LowongCommentHandbookCitation Pointer502948; Journal; Peinemann; ARPMAS; Arch.Pharm.(Weinheim Ger.); 234; 1896; 258;

Derivative (1 of 1)

Derivative BRN288703Derivative1-(5-benzo[1,3]dioxol-5-yl-pentanoyl)-piperidineCitation Pointer5749938; Journal; Jain, A. K.; Sharma, N. D.; Gupta, S. R.; IJSBDB; Indian J.Chem.Sect.B; EN; 25; 1986; 979;

Related Structure (1 of 1)

Citation Pointer3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Crossfile Reference (1 of 4)

NamePiperine, purumCrossfile SourceFlukaExternal Access ID80810

Crossfile Reference (2 of 4)

NamePiperidine, 1-<5-(1,3-benzodioxol-5-yl)-1-oxo-2,4-pentadienyl>-, (E,E)-Crossfile SourceCRC Handbook of Chemistry and PhysicsExternal Access ID20134

Crossfile Reference (3 of 4)

Data Type13C-NMR SpectrumCrossfile SourceCSEARCHExternal Access IDSADT-12317

Crossfile Reference (4 of 4)

Data Type13C-NMR SpectrumCrossfile SourceCSEARCHExternal Access IDUNIW-14585

Crystal Property Description (1 of 2)

Colour & Other Propertieslight-yellowCitation Pointer6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 – 2397;

Crystal Property Description (2 of 2)

Colour & Other PropertiesPrismenCommentHandbookCitation Pointer967610; Journal; Tunmann; CHZEA6; Chem.Zentralbl.; GE; 89; II; 1918; 675;

Melting Point (1 of 19)

Solventethyl acetateCommentHandbookCitation Pointer967610; Journal; Tunmann; CHZEA6; Chem.Zentralbl.; GE; 89; II; 1918; 675;

Melting Point (2 of 19)

Melting Point131Solventdiethyl etherCitation Pointer5749938; Journal; Jain, A. K.; Sharma, N. D.; Gupta, S. R.; IJSBDB; Indian J.Chem.Sect.B; EN; 25; 1986; 979;

Melting Point (3 of 19)

Melting Point132SolventbenzeneCitation Pointer3132150; Journal; Madhusudhana et al.; CUSCAM; Curr.Sci.; 43; 1974; 76;

Melting Point (4 of 19)

Melting Point130Citation Pointer5575872; Journal; Banerji, Avijit; Nandi, Gopa; IJSBDB; Indian J.Chem.Sect.B; EN; 27; 1-12; 1988; 163-165;

Melting Point (5 of 19)

Melting Point130Citation Pointer3143698; Journal; Dhar; Raina; PLMEAA; Planta Med.; 23; 1973; 295,296;

Melting Point (6 of 19)

Melting Point129.5CommentHandbookCitation Pointer502948; Journal; Peinemann; ARPMAS; Arch.Pharm.(Weinheim Ger.); 234; 1896; 258;

Melting Point (7 of 19)

Melting Point129.5CommentHandbookCitation Pointer981397; Journal; Kofler,L.u.A.; Thermo-Mikro-Methoden,3.Aufl.; <Weinheim 1954> S.471;

Melting Point (8 of 19)

Melting Point127Citation Pointer5975360; Journal; Dehmlow, Eckehard V.; Shamout, Abdul Rahman; JRMPDM; J.Chem.Res.Miniprint; GE; 4; 1981; 1178-1184;

Melting Point (9 of 19)

Melting Point129Citation Pointer5874394; Journal; Nakatani, Nobuji; Inatani, Reiko; ABCHA6; Agric.Biol.Chem.; EN; 45; 6; 1981; 1473-1476;

Melting Point (10 of 19)

Melting Point128Citation Pointer5576619; Journal; Banerji, Avijit; Ghosal, Tapasree; Acharyya, Aditi K.; IJSBDB; Indian J.Chem.Sect.B; EN; 23; 6; 1984; 546-549;

Melting Point (11 of 19)

Melting Point129Citation Pointer3143025; Journal; Patra; Gosh; PYTCAS; Phytochemistry; 13; 1974; 2889;3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Melting Point (12 of 19)

Melting Point128Citation Pointer3140982; Journal; Grewe et al.; CHBEAM; Chem.Ber.; 103; 1970; 3752,3766;

Melting Point (13 of 19)

Melting Point128.5 – 130Citation Pointer3714671; Journal; Meerov; Katyuzhanskaya; CHNCA8; Chem.Nat.Compd.(Engl.Transl.); 9; 1973; 179; KPSUAR; Khim.Prir.Soedin.; 9; 1973; 184;

Melting Point (14 of 19)

Melting Point129 – 130Citation Pointer2995721; Patent; Haarmann and Reimer; DE 2757506; 1977;

Melting Point (15 of 19)

Melting Point128 – 129.5Citation Pointer3141492; Journal; Lurik et al.; PCJOAU; Pharm.Chem.J.(Engl.Transl.); 5; 8; 1971; 462; KHFZAN; Khim.Farm.Zh.; 5; 8; 1971; 15;

Melting Point (16 of 19)

Melting Point128 – 130Citation Pointer156361; Journal; Okogun,J.I.; Ekong,D.E.U.; JCPRB4; J.Chem.Soc.Perkin Trans.1; EN; 1974; 2195-2198;

Melting Point (17 of 19)

Melting Point128 – 129.5CommentHandbookCitation Pointer960844; Journal; Ruegheimer; CHBEAM; Chem.Ber.; 15; 1882; 1391;

Melting Point (18 of 19)

Melting Point128 – 129Citation Pointer6070238; Journal; Siddiqui, Bina S.; Begum, Sabira; Gulzar, Tahsin; Noor, Farhat and Fatima; PYTCAS; Phytochemistry; EN; 45; 8; 1997; 1617-1620;

Melting Point (19 of 19)

Melting Point124Citation Pointer6205590; Journal; Pande, Archana; Shukla, Y. N.; Srivastava, Ritu; Verma, Monika; IJSBDB; Indian J.Chem.Sect.B; EN; 36; 4; 1997; 377 – 379;

Crystal Phase (1 of 8)

DescriptionRate of crystallizationCommentvon unterkuehltem Piperin bei verschiedenen Temperaturen.; HandbookCitation Pointer969754; Journal; Tammann; ZEPCAC; Z.Phys.Chem.Stoechiom.Verwandtschaftsl.; 25; 1894; 450; ZAACAB; Z.Anorg.Allg.Chem.; 181; 1929; 413;

Crystal Phase (2 of 8)

DescriptionRate of crystallizationCommentvon unterkuehltem Piperidin bei Drucken bis 1000 kg/cm2.; HandbookCitation Pointer969753; Journal; Hasselblatt; ZAACAB; Z.Anorg.Allg.Chem.; 119; 1921; 361;

Crystal Phase (3 of 8)

DescriptionRate of crystallizationCommentGeschwindigkeit der Bildung von Keimen bei der Kristallisation von unterkuehlten Schmelzen bei 20grad bzw. bei 48grad:.; HandbookCitation Pointer981393; Journal; Kondoguri; ZETFA7; Zh.Eksp.Teor.Fiz.; 11; 1941; 728; Chem.Abstr.; 1943; 1314;2200674; Journal; Michnewitsch; KOZHAG; Kolloidn.Zh.; 21; 1959; 69; engl. Ausg. S. 61;

Crystal Phase (4 of 8)

DescriptionRate of crystallizationCommentKeimbildung bei der Kristallisation von unterkuehlten Schmelzen in Abhaengigkeit von der Temperatur (72-80grad):.; HandbookCitation Pointer2175033; Journal; Tammann; Elsner v. Gronow; ZAACAB; Z.Anorg.Allg.Chem.; 200; 1931; 57, 68;

Crystal Phase (5 of 8)

DescriptionRate of crystallizationCommentin Abhaengigkeit von der Temperatur(0gradbis 90grad) und vom Reinheitsgrad:.; HandbookCitation Pointer981393; Journal; Kondoguri; ZETFA7; Zh.Eksp.Teor.Fiz.; 11; 1941; 728; Chem.Abstr.; 1943; 1314;

Crystal Phase (6 of 8)

DescriptionRate of crystallizationCommentVerstaerkte Keimbildung bei der Kristallisation von unterkuehlten Schmelzen bei Einwirkung von Ultraschall.; HandbookCitation Pointer2175021; Journal; Danilow; Tewerowskii; ZETFA7; Zh.Eksp.Teor.Fiz.; 10; 1940; 1305, 1308; Chem.Abstr.; 1941; 5368;

Crystal Phase (7 of 8)

DescriptionInterplanar spacingCommentvon kristallinem und von fluessigem Piperin:.; HandbookCitation Pointer981396; Journal; Lewaschewitsch et al.; Trudy Dnetropetrovsk.chim.-technol.Inst.; 4; 1955; 84,88; Chem.Abstr.; 1959; 9760;

Crystal Phase (8 of 8)

DescriptionSolid state structure propertiesCitation Pointer3132105; Journal; Grynpas; Lindley; ACBCAR; Acta Crystallogr.Sect.B; 31; 1975; 2663,2664,2665,2666;

Sublimation (1 of 1)

Sublimation104Pressure0.02CommentHandbookCitation Pointer636409; Journal; Janot; Chaigneau; COREAF; C.R.Hebd.Seances Acad.Sci.; 225; 1947; 1371;

Density of the Liquid (1 of 4)

Density of the Liquid1.25Commentg/cm**3Citation Pointer3132105; Journal; Grynpas; Lindley; ACBCAR; Acta Crystallogr.Sect.B; 31; 1975; 2663,2664,2665,2666;

Density of the Liquid (2 of 4)

Density of the Liquid1.192Reference Temperature4Measurement Temperature20CommentHandbookCitation Pointer981390; Journal; Kordes; ZPCBAL; Z.Phys.Chem.Abt.B; 43; 1939; 173,186;

Density of the Liquid (3 of 4)

Density of the Liquid1.13Measurement Temperature113Commentg/cm**3; HandbookCitation Pointer969752; Journal; Tammann; Tampke; ZAACAB; Z.Anorg.Allg.Chem.; 162; 1927; 10;

Density of the Liquid (4 of 4)

Density of the Liquid1.12Measurement Temperature136Commentg/cm**3; HandbookCitation Pointer969752; Journal; Tammann; Tampke; ZAACAB; Z.Anorg.Allg.Chem.; 162; 1927; 10;

Dynamic Viscosity (1 of 1)

Dynamic Viscosity11.3Temperature95CommentHandbookCitation Pointer969749; Journal; Tammann; ZAACAB; Z.Anorg.Allg.Chem.; 181; 1929; 413;969752; Journal; Tammann; Tampke; ZAACAB; Z.Anorg.Allg.Chem.; 162; 1927; 10;969751; Journal; Tammann; Hesse; ZAACAB; Z.Anorg.Allg.Chem.; 156; 1926; 252;

Refractive Index (1 of 1)

Refractive Index1.6846Wavelength589Temperature20CommentHandbookCitation Pointer981390; Journal; Kordes; ZPCBAL; Z.Phys.Chem.Abt.B; 43; 1939; 173,186;

Nuclear Magnetic Resonance (1 of 15)

Coupling Nuclei1H-1HSolventsCDCl3Frequency500Citation Pointer6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 – 2397;

Nuclear Magnetic Resonance (2 of 15)

DescriptionSpectrumNucleus1HTemperature41.9Citation Pointer5945187; Journal; Braumann, Urich; Haendel, heidrun; Albert, Klaus; Ecker, Rainer; Spraul, Manfred; ANCHAM; Anal.Chem.; EN; 67; 5; 1995; 930-935;

Nuclear Magnetic Resonance (3 of 15)

DescriptionChemical shiftsNucleus13CSolventsCDCl3Frequency125.7Citation Pointer6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 – 2397;

Nuclear Magnetic Resonance (4 of 15)

DescriptionChemical shiftsNucleus1HSolventsCDCl3Frequency500Citation Pointer6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 – 2397;

Nuclear Magnetic Resonance (5 of 15)

DescriptionChemical shiftsNucleus1HSolventsCDCl3Citation Pointer6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Nuclear Magnetic Resonance (6 of 15)

DescriptionChemical shiftsNucleus13CSolventsCDCl3Citation Pointer6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Nuclear Magnetic Resonance (7 of 15)

DescriptionChemical shiftsNucleus1HSolventsCDCl3Citation Pointer5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;

Nuclear Magnetic Resonance (8 of 15)

DescriptionChemical shiftsNucleus13CSolventsCDCl3Citation Pointer5787666; Journal; Banerji, Avijit; Sarkar, Manjusha (nee Chaudhuri); Ghosal, Tapasree; Pal, Sudhir Chandra; ORMRBD; Org.Magn.Reson.; EN; 22; 11; 1984; 734-736;

Nuclear Magnetic Resonance (9 of 15)

DescriptionChemical shiftsNucleus1HSolventsCDCl3Citation Pointer5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Nuclear Magnetic Resonance (10 of 15)

DescriptionChemical shiftsNucleus13CSolventsCDCl3Citation Pointer5576619; Journal; Banerji, Avijit; Ghosal, Tapasree; Acharyya, Aditi K.; IJSBDB; Indian J.Chem.Sect.B; EN; 23; 6; 1984; 546-549;5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Nuclear Magnetic Resonance (11 of 15)

Description2D-NMRCitation Pointer5945187; Journal; Braumann, Urich; Haendel, heidrun; Albert, Klaus; Ecker, Rainer; Spraul, Manfred; ANCHAM; Anal.Chem.; EN; 67; 5; 1995; 930-935;

Nuclear Magnetic Resonance (12 of 15)

DescriptionNMRCitation Pointer3143025; Journal; Patra; Gosh; PYTCAS; Phytochemistry; 13; 1974; 2889;3633754; Journal; Wenkert et al.; JACSAT; J.Amer.Chem.Soc.; 93; 1971; 6271;3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Nuclear Magnetic Resonance (13 of 15)

DescriptionSpin-spin coupling constantsSolventsCDCl3Comment1H-1HCitation Pointer5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Nuclear Magnetic Resonance (14 of 15)

DescriptionSpin-spin coupling constantsSolventsCDCl3Comment1H-13C.Citation Pointer5787666; Journal; Banerji, Avijit; Sarkar, Manjusha (nee Chaudhuri); Ghosal, Tapasree; Pal, Sudhir Chandra; ORMRBD; Org.Magn.Reson.; EN; 22; 11; 1984; 734-736;

Nuclear Magnetic Resonance (15 of 15)

DescriptionSpin-spin coupling constantsSolventsCDCl3Comment1H-1HCitation Pointer5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Infrared Spectra (1 of 12)

DescriptionBandsSolventKBrCitation Pointer6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 – 2397;

Infrared Spectra (2 of 12)

DescriptionBandsComment3058 – 1043 cm**(-1)Citation Pointer6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Infrared Spectra (3 of 12)

DescriptionBandsComment1650 – 930 cm**(-1)Citation Pointer5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;

Infrared Spectra (4 of 12)

DescriptionBandsSolventKBrComment1635 – 925 cm**(-1)Citation Pointer5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Infrared Spectra (5 of 12)

DescriptionBandsSolventCHCl3Comment1635 – 1585 cm**(-1)Citation Pointer5725528; Journal; Nakamura, Norio; Kiuchi, Fumiyuki; Tsuda, Yoshisuke; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2647-2651;

Infrared Spectra (6 of 12)

DescriptionBandsSolventKBrComment1635 – 1585 cm**(-1)Citation Pointer5725528; Journal; Nakamura, Norio; Kiuchi, Fumiyuki; Tsuda, Yoshisuke; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2647-2651;

Infrared Spectra (7 of 12)

DescriptionBandsSolventKBrComment1641 – 1624 cm**(-1)Citation Pointer5571390; Journal; Cabre, Juan; Palomo, Antonio Luis; SYNTBF; Synthesis; EN; 5; 1984; 413-417;

Infrared Spectra (8 of 12)

DescriptionBandsSolventnujolComment1600 – 780 cm**(-1); HandbookCitation Pointer642911; Journal; Pleat et al.; JPHAA3; J.Am.Pharm.Assoc.; 40; 1951; 107, 108;

Infrared Spectra (9 of 12)

DescriptionBandsSolventKBrComment3020 – 710 cm**(-1); HandbookCitation Pointer511899; Journal; Briggs et al.; ANCHAM; Anal.Chem.; 29; 1957; 904, 905;

Infrared Spectra (10 of 12)

DescriptionBandsSolventCHCl3Comment1635 – 1580 cm**(-1); HandbookCitation Pointer511899; Journal; Briggs et al.; ANCHAM; Anal.Chem.; 29; 1957; 904, 905;1056240; Journal; Marion et al.; JACSAT; J.Amer.Chem.Soc.; 73; 1951; 305,; JACSAT; J.Amer.Chem.Soc.; 74; 1952; 270;

Infrared Spectra (11 of 12)

DescriptionBandsSolventCHCl3Comment1490 – 930 cm**(-1); HandbookCitation Pointer511899; Journal; Briggs et al.; ANCHAM; Anal.Chem.; 29; 1957; 904, 905;1056240; Journal; Marion et al.; JACSAT; J.Amer.Chem.Soc.; 73; 1951; 305,; JACSAT; J.Amer.Chem.Soc.; 74; 1952; 270;

Infrared Spectra (12 of 12)

DescriptionIRCitation Pointer3132150; Journal; Madhusudhana et al.; CUSCAM; Curr.Sci.; 43; 1974; 76;3143025; Journal; Patra; Gosh; PYTCAS; Phytochemistry; 13; 1974; 2889;

Ultraviolet Spectra (1 of 10)

DescriptionSpectrumSolventCHCl3Comment300 – 400 nm; HandbookCitation Pointer981386; Journal; Tausig et al.; JFOTAP; J.Food Technol.; 10; 1956; 151;

Ultraviolet Spectra (2 of 10)

DescriptionSpectrumSolventethanolComment290 – 380 nm; HandbookCitation Pointer529237; Journal; Spring; Stark; JCSOA9; J.Chem.Soc.; 1950; 1177, 1178;

Ultraviolet Spectra (3 of 10)

DescriptionAbsorption maximaAbsorption Maxima341Ext./Abs. Coefficient20893Citation Pointer5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;

Ultraviolet Spectra (4 of 10)

DescriptionAbsorption maximaSolventmethanolAbsorption Maxima309; 341Citation Pointer5749938; Journal; Jain, A. K.; Sharma, N. D.; Gupta, S. R.; IJSBDB; Indian J.Chem.Sect.B; EN; 25; 1986; 979;

Ultraviolet Spectra (5 of 10)

DescriptionAbsorption maximaSolventmethanolAbsorption Maxima343Ext./Abs. Coefficient34700Citation Pointer5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Ultraviolet Spectra (6 of 10)

DescriptionAbsorption maximaSolventmethanolAbsorption Maxima245; 255; 262; 311Ext./Abs. Coefficient11100; 11200; 11100; 21700Citation Pointer5729448; Journal; Kiuchi, Fumiyuki; Nakamura, Norio; Tsuda, Yoshisuke; Kondo, Kaoru; Yoshimura, Hiroyuki; CPBTAL; Chem.Pharm.Bull.; EN; 36; 7; 1988; 2452-2465;

Ultraviolet Spectra (7 of 10)

DescriptionAbsorption maximaCitation Pointer3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Ultraviolet Spectra (8 of 10)

DescriptionAbsorption maximaCommentdes Dampfes.; HandbookCitation Pointer968116; Journal; Purvis; JCSOA9; J.Chem.Soc.; 103; 1913; 2291;

Ultraviolet Spectra (9 of 10)

DescriptionAbsorption maximaSolventethanolCommentHandbookCitation Pointer505581; Journal; Dobbie; Fox; JCSOA9; J.Chem.Soc.; 103; 1913; 1194;

Ultraviolet Spectra (10 of 10)

DescriptionUV/VISCitation Pointer3132150; Journal; Madhusudhana et al.; CUSCAM; Curr.Sci.; 43; 1974; 76;3140982; Journal; Grewe et al.; CHBEAM; Chem.Ber.; 103; 1970; 3752,3766;3141492; Journal; Lurik et al.; PCJOAU; Pharm.Chem.J.(Engl.Transl.); 5; 8; 1971; 462; KHFZAN; Khim.Farm.Zh.; 5; 8; 1971; 15;3143025; Journal; Patra; Gosh; PYTCAS; Phytochemistry; 13; 1974; 2889;3714671; Journal; Meerov; Katyuzhanskaya; CHNCA8; Chem.Nat.Compd.(Engl.Transl.); 9; 1973; 179; KPSUAR; Khim.Prir.Soedin.; 9; 1973; 184;

Mass Spectrum (1 of 5)

Citation Pointer3140982; Journal; Grewe et al.; CHBEAM; Chem.Ber.; 103; 1970; 3752,3766;3635101; Journal; De Cleyn; Verzele; BSCBAG; Bull.Soc.Chim.Belg.; 84; 1975; 435,436;

Mass Spectrum (2 of 5)

Descriptionspectrum; electron impact (EI)Citation Pointer6311443; Journal; Schobert, Rainer; Siegfried, Sven; Gordon, Gary J.; JCSPCE; J.Chem.Soc.Perkin Trans.1; EN; 19; 2001; 2393 – 2397;

Mass Spectrum (3 of 5)

DescriptionspectrumCitation Pointer5864041; Journal; Dahiya, Jagroop S.; Woods, Donald L.; Tewari, Jalpa P.; PYTCAS; Phytochemistry; EN; 27; 7; 1988; 2366;6090513; Journal; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain; SYNCAV; Synth.Commun.; EN; 28; 2; 1998; 239-250;

Mass Spectrum (4 of 5)

Descriptionspectrum; electron impact (EI)Citation Pointer5825902; Journal; Semler, Ursula; Gross, Georg G.; PYTCAS; Phytochemistry; EN; 27; 5; 1988; 1566-1568;

Mass Spectrum (5 of 5)

Descriptionelectron impact (EI)Citation Pointer5874363; Journal; Nakamura, Masamichi; Katoh, Kuni; Kawabata, Toshiharu; ABCHA6; Agric.Biol.Chem.; EN; 45; 5; 1981; 1257-1260;

Electrical Data (1 of 1)

DescriptionPiezoelectricityCommentHandbookCitation Pointer536898; Journal; Kopzik et al.; VMUNAE; Vestn.Mosk.Univ.; 13; 6; 1958; 91, 94; Chem.Abstr.; 1959; 15673;

Dissociation Exponent (1 of 3)

Dissociation Exponent (pK)14Temperature18MethodconductometricTypeapparentCommentHandbookCitation Pointer625734; Journal; v. Weisse; Meyer-Levy; JCPBAN; J.Chim.Phys.Phys.Chim.Biol.; 14; 1916; 276; CHZEA6; Chem.Zentralbl.; GE; 87; II; 1916; 1030;

Dissociation Exponent (2 of 3)

Dissociation Exponent (pK)12.22Temperature18Typeb/thermodynamicCommentHandbookCitation Pointer740972; Journal; Kolthoff; BIZEA2; Biochem.Z.; 162; 1925; 340; PHJOAV; Pharm.J.; 118; 126; CHZEA6; Chem.Zentralbl.; GE; 98; I; 1927; 2116;

Dissociation Exponent (3 of 3)

Dissociation Exponent (pK)11.72Temperature55Typeb/thermodynamicCommentHandbookCitation Pointer625129; Journal; Arnall; JCSOA9; J.Chem.Soc.; 117; 1920; 837;

Electrochemical Characteristics (1 of 1)

Descriptionpolarographic current/voltage curveCommentHandbookCitation Pointer981382; Journal; Sato; Japan Analyst; 6; 1957; 83; Chem.Abstr.; 1958; 16088;981383; Journal; Hans; Santavy; C.csl.Lekarn.; 59; 1946; 40; Chem.Abstr.; 1948; 3504;

Solubility (MCS) (1 of 8)

Temperature15SolventtrichloroetheneCommentSolubility :9.83 %.; HandbookCitation Pointer559145; Journal; Wester; CHZEA6; Chem.Zentralbl.; GE; 86; I; 1915; 248;

Solubility (MCS) (2 of 8)

Solventaq. pyridineCommentSolubility :11 %.at:20-25 degreeC.; HandbookCitation Pointer505376; Journal; Dehn; JACSAT; J.Amer.Chem.Soc.; 39; 1917; 1400;

Solubility (MCS) (3 of 8)

SolventpyridineCommentSolubility :23 %.; HandbookCitation Pointer505376; Journal; Dehn; JACSAT; J.Amer.Chem.Soc.; 39; 1917; 1400;

Solubility (MCS) (4 of 8)

SolventethanolComment1 part(s) of substance.dissolves in:30 parts of solvent.; HandbookCitation Pointer969748; Journal; Wagenaar; PHWEAW; Pharm.Weekbl.; 66; 1929; 405;

Solubility (MCS) (5 of 8)

SolventethanolComment1 part(s) of substance.dissolves in:1 parts of solvent.in boiling solvent.; HandbookCitation Pointer969748; Journal; Wagenaar; PHWEAW; Pharm.Weekbl.; 66; 1929; 405;

Solubility (MCS) (6 of 8)

SolventethanolComment 100 g solvent dissolves. 6.66 g Substance.at:20-25 degreeC.; HandbookCitation Pointer562634; Journal; Pucher; Dehn; JACSAT; J.Amer.Chem.Soc.; 43; 1921; 1755;

Solubility (MCS) (7 of 8)

Solubility0.04Saturationin solutionTemperature18SolventH2OCommentHandbookCitation Pointer740972; Journal; Kolthoff; BIZEA2; Biochem.Z.; 162; 1925; 340; PHJOAV; Pharm.J.; 118; 126; CHZEA6; Chem.Zentralbl.; GE; 98; I; 1927; 2116;

Solubility (MCS) (8 of 8)

Solubility0.4Saturationin solutionTemperature18Solventaq. HClCommentHandbookCitation Pointer740972; Journal; Kolthoff; BIZEA2; Biochem.Z.; 162; 1925; 340; PHJOAV; Pharm.J.; 118; 126; CHZEA6; Chem.Zentralbl.; GE; 98; I; 1927; 2116;

Boundary Surface Phenomena (MCS) (1 of 1)

DescriptionSurface tensionSolventH2OCommentHandbookCitation Pointer625737; Journal; Zeehuisen; AEPPAE; Naunyn-Schmiedeberg’s Arch.Exp.Pathol.Pharmakol.; 86; 1920; 366; CHZEA6; Chem.Zentralbl.; GE; 91; III; 1920; 668;

Pharmacological Data (1 of 60)

Citation Pointer6318024; Journal; Sunkara, G.; Mada, S. R.; Vobalaboina, V.; PHARAT; Pharmazie; EN; 56; 8; 2001; 640 – 642;

Pharmacological Data (2 of 60)

Citation Pointer6318024; Journal; Sunkara, G.; Mada, S. R.; Vobalaboina, V.; PHARAT; Pharmazie; EN; 56; 8; 2001; 640 – 642;

Pharmacological Data (3 of 60)

Citation Pointer6318024; Journal; Sunkara, G.; Mada, S. R.; Vobalaboina, V.; PHARAT; Pharmazie; EN; 56; 8; 2001; 640 – 642;

Pharmacological Data (4 of 60)

Citation Pointer6318024; Journal; Sunkara, G.; Mada, S. R.; Vobalaboina, V.; PHARAT; Pharmazie; EN; 56; 8; 2001; 640 – 642;

Pharmacological Data (5 of 60)

Citation Pointer6318024; Journal; Sunkara, G.; Mada, S. R.; Vobalaboina, V.; PHARAT; Pharmazie; EN; 56; 8; 2001; 640 – 642;

Pharmacological Data (6 of 60)

Citation Pointer6318024; Journal; Sunkara, G.; Mada, S. R.; Vobalaboina, V.; PHARAT; Pharmazie; EN; 56; 8; 2001; 640 – 642;

Pharmacological Data (7 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (8 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (9 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (10 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (11 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (12 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (13 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (14 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (15 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (16 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (17 of 60)

Citation Pointer6303601; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 3; 2001; 284 – 287;

Pharmacological Data (18 of 60)

Citation Pointer6303567; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 2; 2001; 176 – 179;

Pharmacological Data (19 of 60)

Citation Pointer6303567; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 2; 2001; 176 – 179;

Pharmacological Data (20 of 60)

Citation Pointer6303567; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 2; 2001; 176 – 179;

Pharmacological Data (21 of 60)

Citation Pointer6303567; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 2; 2001; 176 – 179;

Pharmacological Data (22 of 60)

Citation Pointer6303567; Journal; Bajad, Sunil; Bedi, K. L.; Singla, A. K.; Johri, R. K.; PLMEAA; Planta Med.; EN; 67; 2; 2001; 176 – 179;

Pharmacological Data (23 of 60)

Citation Pointer6264052; Journal; Navickiene, Hosana Maria D.; Alecio, Alberto Camilo; Kato, Massuo Jorge; Bolzani, Vanderlan da S.; Young, Maria Claudia M.; Cavalheiro, Alberto Jose; Furlan, Maysa; PYTCAS; Phytochemistry; EN; 55; 2410; 2000; 621 – 626;

Pharmacological Data (24 of 60)

CommentNo effectCitation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (25 of 60)

CommentNo effectCitation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (26 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (27 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (28 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (29 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (30 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (31 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (32 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (33 of 60)

Citation Pointer6261759; Journal; Rauscher, Frederick M.; Sanders, Ruth A.; Watkins, John B.; JBMTFQ; J.Biochem.Mol.Toxicol.; EN; 14; 6; 2000; 329 – 334;

Pharmacological Data (34 of 60)

Citation Pointer6235546; Journal; Daware, Mahadeo B.; Mujumdar, Arvind M.; Ghaskadbi, Surendra; PLMEAA; Planta Med.; EN; 66; 3; 2000; 231 – 236;

Pharmacological Data (35 of 60)

Citation Pointer6235546; Journal; Daware, Mahadeo B.; Mujumdar, Arvind M.; Ghaskadbi, Surendra; PLMEAA; Planta Med.; EN; 66; 3; 2000; 231 – 236;

Pharmacological Data (36 of 60)

Citation Pointer6235546; Journal; Daware, Mahadeo B.; Mujumdar, Arvind M.; Ghaskadbi, Surendra; PLMEAA; Planta Med.; EN; 66; 3; 2000; 231 – 236;

Pharmacological Data (37 of 60)

Citation Pointer6235546; Journal; Daware, Mahadeo B.; Mujumdar, Arvind M.; Ghaskadbi, Surendra; PLMEAA; Planta Med.; EN; 66; 3; 2000; 231 – 236;

Pharmacological Data (38 of 60)

Citation Pointer6235546; Journal; Daware, Mahadeo B.; Mujumdar, Arvind M.; Ghaskadbi, Surendra; PLMEAA; Planta Med.; EN; 66; 3; 2000; 231 – 236;

Pharmacological Data (39 of 60)

Citation Pointer6224648; Journal; Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant; BMECEP; Bioorg.Med.Chem.; EN; 8; 1; 2000; 251 – 268;

Pharmacological Data (40 of 60)

Citation Pointer6224648; Journal; Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant; BMECEP; Bioorg.Med.Chem.; EN; 8; 1; 2000; 251 – 268;

Pharmacological Data (41 of 60)

Citation Pointer6224648; Journal; Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant; BMECEP; Bioorg.Med.Chem.; EN; 8; 1; 2000; 251 – 268;

Pharmacological Data (42 of 60)

Citation Pointer6224648; Journal; Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant; BMECEP; Bioorg.Med.Chem.; EN; 8; 1; 2000; 251 – 268;

Pharmacological Data (43 of 60)

Citation Pointer6224648; Journal; Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant; BMECEP; Bioorg.Med.Chem.; EN; 8; 1; 2000; 251 – 268;

Pharmacological Data (44 of 60)

Citation Pointer6221629; Journal; Kuenzi, Frederick M.; Dale, Nicholas; BJPCBM; Br.J.Pharmacol.; EN; 119; 1; 1996; 81 – 90;

Pharmacological Data (45 of 60)

Citation Pointer6202145; Journal; Chu, C.- Y.; Chang, J.-P.; Wang, C.-J.; FCTOD7; Food Chem.Toxicol.; EN; 32; 4; 1994; 373 – 378;

Pharmacological Data (46 of 60)

Citation Pointer6202145; Journal; Chu, C.- Y.; Chang, J.-P.; Wang, C.-J.; FCTOD7; Food Chem.Toxicol.; EN; 32; 4; 1994; 373 – 378;

Pharmacological Data (47 of 60)

Citation Pointer6199610; Journal; Kang, Min Hee; Won, Sun Me; Park, Sang Shin; Kim, Sang Geon; Novak, R. F.; Kim, Nak Doo; XENOBH; Xenobiotica; EN; 24; 12; 1994; 1195 – 1204;

Pharmacological Data (48 of 60)

Citation Pointer6188824; Journal; Unchern, Surachai; Saito, Hiroshi; Nishiyama, Nobuyoshi; BPBLEO; Biol.Pharm.Bull.; EN; 20; 9; 1997; 958 – 961;

Pharmacological Data (49 of 60)

Citation Pointer6143346; Journal; Wink, M.; Schmeller, T.; Latz-Bruening, B; JCECD8; J.Chem.Ecol.; EN; 24; 11; 1998; 1881 – 1938;

Pharmacological Data (50 of 60)

Citation Pointer6143346; Journal; Wink, M.; Schmeller, T.; Latz-Bruening, B; JCECD8; J.Chem.Ecol.; EN; 24; 11; 1998; 1881 – 1938;

Pharmacological Data (51 of 60)

Citation Pointer6143346; Journal; Wink, M.; Schmeller, T.; Latz-Bruening, B; JCECD8; J.Chem.Ecol.; EN; 24; 11; 1998; 1881 – 1938;

Pharmacological Data (52 of 60)

Citation Pointer6143346; Journal; Wink, M.; Schmeller, T.; Latz-Bruening, B; JCECD8; J.Chem.Ecol.; EN; 24; 11; 1998; 1881 – 1938;

Pharmacological Data (53 of 60)

CommentNo effectCitation Pointer6143346; Journal; Wink, M.; Schmeller, T.; Latz-Bruening, B; JCECD8; J.Chem.Ecol.; EN; 24; 11; 1998; 1881 – 1938;

Pharmacological Data (54 of 60)

CommentNo effectCitation Pointer6143346; Journal; Wink, M.; Schmeller, T.; Latz-Bruening, B; JCECD8; J.Chem.Ecol.; EN; 24; 11; 1998; 1881 – 1938;

Pharmacological Data (55 of 60)

CommentNo effectCitation Pointer6143346; Journal; Wink, M.; Schmeller, T.; Latz-Bruening, B; JCECD8; J.Chem.Ecol.; EN; 24; 11; 1998; 1881 – 1938;

Pharmacological Data (56 of 60)

Citation Pointer6132209; Journal; Singh, Amar; Sharma, S. C.; Zutshi, Usha; Bedi, K. L.; PHSCFB; Pharm.Sci.; EN; 3; 4; 1997; 189 – 192;

Pharmacological Data (57 of 60)

Commentin vitro anti-invasive activity against MCF-7/6 cells: anti-invasive at a dose 100 mM, not anti-invasive at a dose 1 mM and 10 mMCitation Pointer6073861; Journal; Parmar, Virinder S.; Bracke, Marc E.; Philippe, Jan; Wengel, Jesper; Jain, Subhash C.; et al.; BMECEP; Bioorg.Med.Chem.; EN; 5; 8; 1997; 1609-1620;

Pharmacological Data (58 of 60)

Commentno effect on the induction of histidine revertants in Salmonella typhimurium in 10 – 500 nmol/plate; no mutagenic effect in the bone marrow micronucleus test in Swiss mice in 10 – 20 mg/kg dose; did not induce any aberration in the sperm cellsCitation Pointer6061215; Journal; Karekar, Varsha R.; Mujumdar, Arvind M.; Joshi, Savita S.; Dhuley, Jayant; Shinde, Sambhaji L.; Ghaskadbi, Surendra; ARZNAD; Arzneim.Forsch.; EN; 46; 10; 1996; 972-975;

Pharmacological Data (59 of 60)

Commentno insecticidal activity against Callosobruchus chinensis L.Citation Pointer5942128; Journal; Miyakado, Masakazu; Nakayama, Isamu; Yoshioka, Hirosuke; ABCHA6; Agric.Biol.Chem.; EN; 44; 7; 1980; 1701-1704;

Pharmacological Data (60 of 60)

Commenttoxicity to mosquito larvae (Culex Spp.); LC50Citation Pointer5510783; Journal; Das, B. P.; Jamal, Molla Yousuf; Choudhury, B.; JICSAH; J.Indian Chem.Soc.; EN; 67; 1; 1990; 72-73;