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Synthesis of p-Methoxyphenylacetone by Psycho Chemist Procedure In a 1000 mL flask with double surface condenser/drierite tube, reflux 600 mL acetic anhydride, 100 mL pyridine (dry) and 100 g 4-methoxyphenylacetic acid for 18 hrs with good
Ephedrine Reduction with HI/P by Wizard X [ Back to the Chemistry Archive ] 57% HI Solution (Hydriodic Acid): Boiling point 125.5-126.5 deg C Density 1.70 gr/ml 55-57% w/w HI is 0.936 to 0.99 grams of HI per ml. Reaction: H2S + I2 ===>> 2HI
This is a convenient way of making a 10% methanolic solution of methylamine freebase from the commercially available 40% aqueous solution. Put in a 2-neck flask 700 grams of commercial dry NaOH, and using a compensating pressure separatory